Advanced Practical Organic Chemistry
Advanced Practical Organic Chemistry
This book is written for advanced undergraduate and graduate students as well as industrial organic chemists, particularly those involved in pharmaceutical, agrochemical, and other areas of fine chemical research. It provides the novice or nonspecialist with the often difficult-to-find information on reagent properties needed to perform general techniques. With over 80 years combined experience training and developing organic research chemists in industry and academia, the authors offer sufficient guidance for researchers to perform reactions under conditions that give the highest chance of success, including the appropriate precautions to take and proper experimental protocols. The text also covers the following topics:
Record keeping and equipment
Solvent purification and reagent preparation
Using gases and working with vacuum pumps
Purification, including crystallization and distillation
Small-scale and large-scale reactions
Characterization, including NMR spectra, melting point and boiling point, and microanalysis
Efficient ways to find information in the chemical literature
With fully updated text and all newly drawn figures, the third edition provides a powerful tool for building the knowledge on the
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This book is written for advanced undergraduate and graduate students as well as industrial organic chemists, particularly those involved in pharmaceutical, agrochemical, and other areas of fine chemical research. It provides the novice or nonspecialist with the often difficult-to-find information on reagent properties needed to perform general techniques. With over 80 years combined experience training and developing organic research chemists in industry and academia, the authors offer sufficient guidance for researchers to perform reactions under conditions that give the highest chance of success, including the appropriate precautions to take and proper experimental protocols. The text also covers the following topics:
Record keeping and equipment
Solvent purification and reagent preparation
Using gases and working with vacuum pumps
Purification, including crystallization and distillation
Small-scale and large-scale reactions
Characterization, including NMR spectra, melting point and boiling point, and microanalysis
Efficient ways to find information in the chemical literature
With fully updated text and all newly drawn figures, the third edition provides a powerful tool for building the knowledge on the
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